Hach Polymetron 9611sc Maintenance And Troubleshooting Manual

DOC023.98.80249

Polymetron 9610sc/9611sc

07/2016, Edition 3

Maintenance and Troubleshooting

Wartung und Fehlerbehebung

Manutenzione e risoluzione dei problemi

Maintenance et dépannage

Mantenimiento y solución de problemas

Manutenção e resolução de problemas

Údržba a odstraňování problémů

Vedligeholdelse og fejlfinding

Onderhoud en probleemoplossing

Konserwacja i usuwanie usterek

Underhåll och felsökning

Huolto ja vianmääritys

Поддръжка и Oтстраняване на проблеми

Karbantartás és hibaelhárítás

Întreţinerea şi depanarea

Techninė priežiūra ir trikčių šalinimas

Техническое обслуживание и устранение неполадок

Bakım ve Sorun Giderme

Údržba a riešenie problémov

Vzdrževanje in odpravljanje težav

Održavanje i rješavanje problema

Συντήρηση και αντιμετώπιση προβλημάτων

Hooldus ja tõrkeotsing

English..............................................................................................................................3

Deutsch.......................................................................................................................... 18

Italiano............................................................................................................................ 35

Français......................................................................................................................... 52

Español.......................................................................................................................... 69

Português...................................................................................................................... 86

Čeština......................................................................................................................... 103

Dansk............................................................................................................................119

Nederlands................................................................................................................. 136

Polski............................................................................................................................ 152

Svenska....................................................................................................................... 168

Suomi............................................................................................................................184

български................................................................................................................... 200

Magyar......................................................................................................................... 217

Română....................................................................................................................... 234

lietuvių kalba...............................................................................................................250

Русский........................................................................................................................266

Türkçe...........................................................................................................................283

Slovenský jazyk......................................................................................................... 299

Slovenski..................................................................................................................... 315

Hrvatski........................................................................................................................ 331

Ελληνικά...................................................................................................................... 347

eesti keel..................................................................................................................... 364

2

Table of contents

Maintenance schedule on page 3 Replace the analyzer bottles on page 7

Put the analyzer in shutdown mode on page 4 Troubleshooting on page 10

Clean the instrument on page 4 Replacement parts and accessories on page 15

Safety information

Refer to the installation user manual for general safety information, hazard descriptions and

precautionary labels descriptions.

Maintenance

D A N G E R

Multiple hazards. Only qualified personnel must conduct the tasks described in this section of the

document.

Maintenance schedule

Table 1 shows the recommended schedule of maintenance tasks. Facility requirements and

operating conditions may increase the frequency of some tasks.

Table 1 Maintenance schedule

Task 30 days 60 days 90 days 365 days

Clean external surfaces (Clean the instrument

on page 4).

X

Clean the sample cell (Clean the sample cell

on page 5).

X or as needed

Replace the reagents (Replace the analyzer bottles

on page 7).

X

1

X

2

Replace the standards (Replace the analyzer bottles

on page 7).

X

3

Clean or replace the sample (y-strainer) filter X or as needed

Replace the fan filter X or as needed

Replace the reagent air filter X

Replace the tubing X

Replace the stir bar X

Replace the sample cell X

1

With 10 minute cycles

2

With 15 minute cycles

3

With one calibration per week

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View maintenance information

Use the service menu to view or reset the service history for the instrument parts.

1. Push diag.

2. Select SERVICE.

3. Select an option.

Option Description

SERVICE PART Shows a list of parts and the date of the last service, the date of the next service and

the number of days before the next service is due. Restart the counter for the next

service.

PART INFORMATION Shows the date when each part was put into service and the total time that each part

has been in use. Some parts include additional information.

UPCOMING SERVICE Shows the name of the service part, the date of the last service, the date of the next

service and the number of days before the next service is due.

SERVICE HISTORY Shows the type, date and time of the last service.

Put the analyzer in shutdown mode

Stop the analyzer before maintenance tasks are started. When the analyzer is stopped, the

colorimeter cell is flushed, then the sample flow, mixer motor, air pump and heater turn off. The

controller menus stay active.

1. Push menu.

2. Select STOP ANALYZER, then YES to confirm.

Note: If START ANALYZER is shown, the analyzer is already in shutdown mode.

3. Wait for the status to show 100% completion.

4. Close the shut-off valves in the sample lines, then complete the maintenance task(s).

Put the analyzer back into operation

After maintenance tasks are complete, start the analyzer.

1. Make sure that all the tubing is connected and that the lower door is closed and latched.

2. Open the shut-off valves in the sample lines.

3. Push menu.

4. Select START ANALYZER.

The analyzer starts normal operation.

Clean the instrument

N O T I C E

Never use cleaning agents such as turpentine, acetone or similar products to clean the instrument including the

display and accessories.

Clean the exterior of the instrument with a moist cloth and a mild soap solution.

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English

Clean spills

C A U T I O N

Chemical exposure hazard. Dispose of chemicals and wastes in accordance with local, regional and

national regulations.

1. Obey all facility safety protocols for spill control.

2. Discard the waste according to applicable regulations.

Sample line and valve cleanup

C A U T I O N

Chemical exposure hazard. Obey laboratory safety procedures and wear all of the personal protective

equipment appropriate to the chemicals that are handled. Refer to the current safety data sheets

(MSDS/SDS) for safety protocols.

New tubing, valves and other sample conditioning equipment may be contaminated with silicate-

based substances (oils, dust). These may contribute to slightly high readings until they are cleaned.

1. Flush the sample line with sample for one to two hours.

2. For an expedient procedure, inject one to four liters of a dilute caustic solution such as 1N (5%)

sodium hydroxide solution into the front end of the sample line. Force the solution through the

analyzer to clean sample system components.

Clean the sample cell

C A U T I O N

Chemical exposure hazard. Obey laboratory safety procedures and wear all of the personal protective

equipment appropriate to the chemicals that are handled. Refer to the current safety data sheets

(MSDS/SDS) for safety protocols.

Put the analyzer in shutdown mode. Refer to Put the analyzer in shutdown mode on page 4.

Clean the sample cell in the colorimeter as needed. Refer to Figure 1 and Figure 2.

Items to collect:

• Cotton swabs, wooden or paper. Do not use swabs with plastic sticks.

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5

Figure 1 Funnel and colorimeter access

Figure 2 Clean the sample cell and stir bar

6 English

Clean the grab sample funnel

Clean the grab sample funnel before and after each use. Refer to Figure 3.

Figure 3 Clean the grab sample funnel

Replace the analyzer bottles

C A U T I O N

Chemical exposure hazard. Obey laboratory safety procedures and wear all of the personal protective

equipment appropriate to the chemicals that are handled. Refer to the current safety data sheets

(MSDS/SDS) for safety protocols.

C A U T I O N

Chemical exposure hazard. Dispose of chemicals and wastes in accordance with local, regional and

national regulations.

Replace the reagent(s) or standard(s) before the level in the analyzer bottle(s) is less than 10%.

1. Put the analyzer in shutdown mode. Refer to Put the analyzer in shutdown mode on page 4.

2. When the status shows 100% completion, open the lower door.

3. Remove the cap from the reagent(s) or standard(s), then remove the bottle(s) from the analyzer.

4. Flush the interior of the analyzer bottle(s) with deionized water.

5. Fill the bottles with fresh reagent(s) or standard(s). Refer to the operations manual.

6. Install the new analyzer bottle(s) and close the lower door. Refer to the operations manual.

7. Push menu and go to REAGENTS/STANDARDS.

8. Select RESET REAGENT LEVELS or RESET STANDARD LEVELS.

9. Select ENTER BLANK VALUE and enter the blank value from Reagent 1.

10. For reagents, select PRIME REAGENTS and confirm.

11. When the reagent prime is complete, start the analyzer. Refer to Put the analyzer back into

operation on page 4.

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7

Replace the fuses

D A N G E R

Electrocution hazard. Always remove power to the instrument before making electrical connections.

D A N G E R

Fire hazard. Use the same type and current rating to replace fuses.

Refer to Figure 4 and Figure 5 to replace the fuses.

Fuse specifications:

Relay fuse: T 5.0 A, 250 V

Output power fuse: AC: T 5.0 A, 250 VAC; DC: T 1.6 A, 250 VAC

Input power fuse: AC: T 1.6 A, 250 VAC; DC: T 6.3 A, 250 VAC

Figure 4 Access cover removal

8 English

Figure 5 Replace the fuses (continued)

1 Relay fuse (4x) 2 Output power fuse (2x) 3 Input power fuse (2x)

Prepare the analyzer for storage

C A U T I O N

Chemical exposure hazard. Obey laboratory safety procedures and wear all of the personal protective

equipment appropriate to the chemicals that are handled. Refer to the current safety data sheets

(MSDS/SDS) for safety protocols.

Remove all the fluids and the power from the analyzer for long-term storage.

1. Put the analyzer in shutdown mode. Refer to Put the analyzer in shutdown mode on page 4.

2. Stop the flow of sample to the analyzer.

3. Remove the reagent and standard solution bottles and pour the solutions into an applicable drain.

4. Flush and fill the bottles with deionized water.

5. Install the bottles and complete a prime cycle two times.

6. Remove the bottles and pour the solutions into an applicable drain.

7. Install the empty bottles and complete a prime cycle two times.

8. Make sure that all the liquid is drained from the colorimeter and tubing.

9. Set the power switch to off.

10. Clean the bottom enclosure.

Update the firmware

Use an SD card with an upgrade file to update the firmware for the controller, sensor or network card.

The upgrade menu is shown only when the SD card contains an upgrade file.

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9

1. Install the SD card into the SD card slot.

2. Select SD CARD SETUP from the MAIN MENU.

Note: The SD CARD SETUP option shows only when an SD card is installed.

3. Select UPGRADE SOFTWARE and confirm. Select the device and upgrade version, if applicable.

4. When the upgrade is complete, the display shows TRANSFER COMPLETE. Remove the SD

card.

5. Restart the instrument for the upgrade to take effect.

Troubleshooting and diagnostics

Troubleshooting

Problem Possible cause Solution

Calibration error The value of the calibration solution in

the calibration menu is different from the

value on the calibration solution bottle.

Change the calibration solution value in the

calibration menu to show the value that is on the

calibration solution bottle.

There is a leak in one of the reagent

delivery valves.

Complete the diagnostic test for reagent delivery

valves. Refer to Diagnostic test for reagent delivery

valves on page 11. If a leak is found, replace the

applicable reagent delivery valve.

The quantity of reagent that is supplied

to the sample cell is incorrect.

Complete the diagnostic test for reagent delivery.

Refer to Diagnostic test for reagent delivery

on page 11. If the reagent delivery is incorrect,

look for a blockage in the tubing or replace the

applicable solenoid valve.

The quantity of calibration solution that

is supplied to the sample cell is

incorrect.

Complete the diagnostic test for calibration solution

delivery. Refer to Diagnostic test for calibration

solution delivery on page 12. If the calibration

solution delivery is incorrect, look for a blockage in

the tubing or replace the applicable solenoid valve.

The stir bar is not installed correctly or

does not move.

Note: The stir bar moves intermittently during

measurements.

Install the stir bar. Make sure that the stir bar moves

during measurements.

The instrument

reading is low or

less than zero.

There is a leak in one of the reagent

delivery valves.

Complete the diagnostic test for reagent delivery

valves. Refer to Diagnostic test for reagent delivery

valves on page 11. If a leak is found, replace the

applicable reagent delivery valve.

The stir bar is not installed correctly or

does not move.

Note: The stir bar moves intermittently during

measurements.

Install the stir bar. Make sure that the stir bar moves

during measurements.

The quantity of reagent that is supplied

to the sample cell is incorrect.

Complete the diagnostic test for reagent delivery.

Refer to Diagnostic test for reagent delivery

on page 11. If the reagent delivery is incorrect,

look for a blockage in the tubing or replace the

applicable solenoid valve.

The reagent blank value in the

REAGENTS/STANDARDS menu is

different from the value on the

R1 (molybdate reagent) bottle.

Change the reagent blank value in the

REAGENTS/STANDARDS menu to show the value

that is on the R1 reagent bottle.

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Problem Possible cause Solution

The instrument

reading is high.

There is a leak in one of the reagent

delivery valves.

Complete the diagnostic test for reagent delivery

valves. Refer to Diagnostic test for reagent delivery

valves on page 11. If a leak is found, replace the

applicable reagent delivery valve.

The quantity of reagent that is supplied

to the sample cell is incorrect.

Complete the diagnostic test for reagent delivery.

Refer to Diagnostic test for reagent delivery

on page 11. If the reagent delivery is incorrect,

look for a blockage in the tubing or replace the

applicable solenoid valve.

The reagent blank value in the

REAGENTS/STANDARDS menu is

different from the value on the

R1 (molybdate reagent) bottle.

Change the reagent blank value in the

REAGENTS/STANDARDS menu to show the value

that is on the R1 reagent bottle.

There is a blue stain on the sample cell. Replace the sample cell. Use the reagent set with

the modified R2 (citric acid) reagent.

The instrument

readings are not

stable.

There is a leak in one of the reagent

delivery valves.

Complete the diagnostic test for reagent delivery

valves. Refer to Diagnostic test for reagent delivery

valves on page 11. If a leak is found, replace the

applicable reagent delivery valve.

The quantity of reagent that is supplied

to the sample cell is incorrect.

Complete the diagnostic test for reagent delivery.

Refer to Diagnostic test for reagent delivery

on page 11. If the reagent delivery is incorrect,

look for a blockage in the tubing or replace the

applicable solenoid valve.

There are bubbles in the sample cell. Look for bubbles in the sample cell. If there are

bubbles in the sample cell, rinse the sample cell. If

the readings do not become stable, replace the

sample cell.

There are bubbles on the stir bar. Look for bubbles on the stir bar. If there are bubbles

on the stir bar, replace the stir bar.

There is a blue stain on the sample cell. Replace the sample cell. Use the reagent set with

the modified R2 (citric acid) reagent.

Reagent

pressure is low.

A bottle cap is not on tightly or does not

make a good seal.

Remove the bottle caps. Clean the rim of the

bottles. Examine the inner surfaces of the bottle

caps for unwanted material. Fully tighten the bottle

caps on the bottles. Make sure the fittings are tight

on top of the bottle caps.

There is a leak or a bad seal in one of

the reagent bottles or tubes.

Complete the diagnostic test for low reagent

pressure. Refer to Diagnostic test for low reagent

pressure on page 12.

Diagnostic test for reagent delivery valves

1. Remove power to the analyzer. Keep the sample and reagent bottles pressurized.

2. Remove the cover from the sample cell.

3. Dry the tubes that are attached to the sample cell cover.

4. Hold the sample cell cover above a dry towel for a minimum of 10 minutes. Make sure that the

tubes do not touch the towel.

5. After 10 minutes, look for fluid to fall from a tube. If fluid falls from a tube, there is a leak in the

valve that is plumbed to the tube.

Diagnostic test for reagent delivery

1. Push diag, then select PERFORM TEST>REAGENT DELIVERY.

2. Set each reagent valve to supply 2000 µL (2 mL).

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3. Collect the reagent from each valve.

4. Measure the volume that was collected.

5. If one valve dispenses less volume than the other valves, look for a blockage in the tubing or

valve.

6. If one valve dispenses more volume than the other valves, replace the valve. Make sure that the

reagent pressure is correct.

Diagnostic test for calibration solution delivery

1. Push diag, then select PERFORM TEST>CAL SOL. DELIVERY.

2. Set the calibration solution valve(s) to supply solution for 1 minute (60 seconds).

3. Collect the calibration solution from the valve(s).

4. Measure the volume that was collected.

5. Compare the measured volume to the specified volume for 1 minute: 55 mL to 300 mL.

Note: The volume collected in 1 minute is the flow rate.

6. If the measured volume is not between 55 mL and 300 mL, replace the applicable valve.

Diagnostic test for low reagent pressure

1. Put the analyzer in shutdown mode. Refer to Put the analyzer in shutdown mode on page 4.

2. Push diag, then select PERFORM TEST>AIR PUMP.

3. Change the settings that follow.

• SETPOINT: 4.00 psi

• LOW DEADBAND: 0.00 psi

• HIGH DEADBAND: 1.00 psi

• SET LOW VALUE: 5.00 psi

• SET HIGH VALUE: 6.00 psi

4. Select START. The test starts. The reagent bottles become fully pressurized.

5. Monitor how frequently the air pump operates during a 5-minute period.

6. If the air pump operates only one time in 5 minutes, the reagent pressure is good. Put the

analyzer back into operation.

7. If the air pump operates more than one time during a 5-minute period, stop the test and complete

the steps that follow.

a. Open the lower door.

b. Fully tighten the caps on the reagent bottles and compression nuts.

c. Make sure that all of the tubes are installed correctly.

d. Make sure that the air manifold fittings are installed correctly and are fully tightened.

e. Close the lower door.

f. Start the air pump test again.

g. If the air pump operates more than one time in 5 minutes, more inspection is necessary.

Diagnostic indicators

The display background and the status indicator light will change to red when an error occurs and to

yellow when a warning occurs.

• Error—red display background and status indicator light. A significant problem occurred that

affects the instrument operation. The current measurement stops and the analyzer goes into

shutdown mode.

• Warning—yellow display background and status indicator light. An event occurred that can cause

a future problem. The analyzer continues to operate.

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English

• Reminders—wrench symbol shows on the display and yellow status indicator light. The time for a

maintenance task has passed.

1. Push diag to access the DIAG/TEST menu.

2. Select an option.

Option Description

DIAGNOSTICS Shows the errors and warnings that currently are on the instrument or on the installed

modules. The analyzer is in operation with the active warnings or reminders until they

are acknowledged or reset. Then, the display background will return to white.

PROGNOSYS Shows the variables which trigger the service indicator and the measurement health

indicator on the display.

CURRENT STATUS Shows the current instrument statuses that follow: OPERATION—Current

measurement mode. SAMPLE CHANNEL—Current sample channel. STEP STATUS

—Current step in the measurement cycle. STEP TIME—Step time remaining.

MINUTES LEFT—Minutes left in current step. COMPLETION—% completed of the

measurement cycle.

ANALYZER HELP Shows all possible errors, warnings and reminders with troubleshooting hints.

PERFORM TEST Examines individual parts of the analyzer. Refer to Start an analyzer test on page 14

for more details about the individual test options.

OUTPUTS Shows the current status of the 4–20 mA and relay outputs with the options to

examine, hold and simulate the outputs. Refer to Output options on page 13 for more

information.

VIEW LED Illuminates the colorimeter cell for improved viewing during troubleshooting. The cell

can be illuminated from 1 to 999 seconds.

MODBUS STATS Shows the status of the Modbus ports: sensor, controller, network and service. Shows

the number of good and bad transmissions.

SERVICE Shows the service parts information and the history. SERVICE PART—shows the last

and the next service date and the remaining days. PART INFORMATION—Shows the

replaced part and the current run time. UPCOMING SERVICE—Shows the next part

which needs to be replaced. SERVICE HISTORY—Shows the date and time of the

replaced parts.

SYSTEM DATA Shows the system information. TEMPERATURE—Shows the measured temperature

of the A/D device in Celsius (C). POWER SOURCE FREQUENCY—Shows the line

power frequency (Hz). POWER SOURCE VOLTAGE—Shows the line power voltage

(V). 12 V VOLTAGE—Shows the measured power supply voltage (V DC). 3.3 V

VOLTAGE—Shows the measured regulated 3.3 V supply (V DC). 12 V CURRENT—

Shows the measured 12 V power supply current (Amps).

I2C DATA Shows the display information (I

2

C) and the version number.

OVERFEED RESET Resets the overfeed timer.

Output options

The output menu shows the current status of the 4–20 mA and relay outputs with the options to

examine, hold and simulate the outputs.

1. Push diag and select OUTPUTS.

2. Select an option.

Option Description

TEST 4–20 mA Examines the 4–20 mA outputs from 1–4.

TEST RELAY Examines the relays A–D. Sets the relays to on or off.

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Option Description

HOLD OUTPUTS Sets the value that the controller sends to an external system for a defined period of

time. After this time period, the instrument reports again real time values. ACTIVATION

—Launches or releases. SET OUTMODE—Hold Outputs (default) or Transfer Outputs.

SET CHANNELS—All (default) or analyzer.

OUTPUT

STATUS

Shows the current status outputs 1–4.

SIMULATE

MEASURE

Shows only when a sensor or module is connected. After the sim value is entered, the

controller outputs this value as if it was the value sent from the sensor. The simulation

stops after the user exits the screen. SELECT SOURCE—Select the module. The footer

shows the current selected source. SET PARAMETER—Sets the parameter for the

source measurement. The footer shows the current selected source. SET SIM VALUE—

Enter the sim value. The footer shows the entered value.

Diagnostic messages

1. When an indicator is shown, push diag, select DIAGNOSTICS, then push enter.

2. Select the error message. The user can acknowledge the error or go to the help screen.

3. To acknowledge the error:

1. Push diag, then select DIAGNOSTICS.

2. Select the error, then push enter.

3. Select ACKNOWLEDGE, then push enter.

4. To go to the help screen:

1. Push diag, then select DIAGNOSTICS.

2. Select the error, then push enter.

3. Select VIEW HELP, then push enter.

Get troubleshooting help

The help screen gives a definition of error, warning or reminder messages and can give associated

tasks to correct the problem.

1. Push diag, then select ANALYZER HELP.

2. Select ERRORS, WARNINGS or REMINDERS.

3. Select one of the topics from the help menu.

Start an analyzer test

The user can complete tests to check the analyzer operation.

1. Push diag, then select PERFORM TEST.

2. Select an option.

Option Description

REAGENT DELIVERY Set each reagent valve to on for a time delivery (50 milliseconds to 65 seconds)

or for a volume delivery (20 to 9,999 µL).

SAMPLE DELIVERY Set each sample valve to on for a sample delivery of 1 to 9999 seconds.

CAL SOL. DELIVERY Set the cal std valve to on for a calibration solution delivery into the colorimeter

cell. Set the duration on from 1 to 9999 seconds.

MIXER Set to on for a clockwise or counterclockwise (CCW/CW) rotation. The revolution

per minute (RPM) can be set from 10 to 500 rpm. On time can be set from 1 to

9999 seconds.

14 English

Option Description

COLORIMETER

HEATER

Set the colorimeter heater settings from 20–60 °C (68–140 °F). The measured

value is shown.

SAMPLE HEATER Set the sample heater settings from 20–60 °C (68–140 °F). The measured value

is shown.

COLORIMETER Start an automatic test which increases the optical LED duty cycle in 5%

increments. This starts from 0% until the output reaches the saturation. The A2D

counts are shown for 0%, then % before the saturation and the first saturation

value (%).

STATUS LED Examine the front panel status LED indicator. The test cycles continuously until

interrupted: off, red, green, yellow.

A2D Set the colorimeter LED intensity to examine the cell transmittance for the A2D

output.

AIR PUMP Change and control the air pressure. SET SETPOINT—Range: 1–9.99 psi. LOW

and HIGH DEADBAND—Range: 0–1 psi. SET LOW and HIGH VALUE—Range:

5–99.99 psi. START—Start the air pump with the entered settings.

FAN Set to adjust the fan duty cycle.

ANALYZER TYPE For use by manufacturer technical support only.

SELECT SCRIPT Toggle between normal instrument script and test script.

SET CHANNELS For use by manufacturer technical support only.

Replacement parts and accessories

W A R N I N G

Personal injury hazard. Use of non-approved parts may cause personal injury, damage to the

instrument or equipment malfunction. The replacement parts in this section are approved by the

manufacturer.

Note: Product and Article numbers may vary for some selling regions. Contact the appropriate distributor or refer to

the company website for contact information.

Replacement parts

Description Item no.

Air pump filter 2718

Bottle, reagent, 2 liter 9395000

Bottle assembly kit, 5 bottles 2037601

Capillary assembly, silica 6786901

Capillary assembly, HR and LR phosphate 6786902

Cell cap 6767800

Cell shroud 6773100

Colorimeter assembly, silica 6786800

Colorimeter assembly, LR phosphate 6786801

Colorimeter assembly, HR phosphate 6786802

Colorimeter cell 6768000

Colorimeter cover 6766900

Fan assembly 6789800

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Replacement parts (continued)

Description Item no.

Fan filter plug 6789300

Fan filter replacement kit 6789100

Funnel, colorimeter 6767100

Funnel cover, colorimeter 6773500

Funnel, reagent bottle 2264472

Fuse, 1.6 A, 250 V, 5 x 20 mm 5208300

Fuse, 5 A, 250 V, slow-blow, 5 x 20 mm 4693800

Heater, sample, for 120/240 VAC instruments 9391700

Heater, sample, for 24 VDC instruments 9391800

Kit, Installation 6783500

Kit, Maintenance, HR phosphate, single channel 6788309

Kit, Maintenance, HR phosphate, two/four channel 6788310

Kit, Maintenance, LR phosphate, single channel 6788307

Kit, Maintenance, LR phosphate, two/four channel 6788308

Kit, Maintenance, silica, single channel 6788304

Kit, Maintenance, silica, two/four channel 6788305

Kit, Maintenance, silica, six channel 6788306

Kit, Sequencer line installation, two channel 6785102

Kit, Sequencer line installation, four channel 6785104

Kit, Sequencer line installation, six channel 6785106

Leak detector board 6562800

Plug, air manifold 014659

Power cord, North American 9179700

Pressure regulator 6782900

Pump, air, assembly 6784500

Reagent bottle tray 9640400

Stir bar 6772600

Tool, flangeless nut extender 5117400

Valve, air relief 6783700

Valve, reagent delivery 6783700

Valve, grab sample 6794300

Valve, pinch, sample, only for instruments with sequencers 6786400

Valve assembly, pinch, for use with any of chemistry standards 6786300

Valve assembly, sample, single channel analyzer 6786500

Y strainer 6784800

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Accessories

Description Quantity Item no.

Panel mount adaptor kit to replace 921x with 5500sc, 9610sc or

9611sc

1 6787100

Sample cooler 1 1757700

Sample conditioning kit, stainless steel 6786600

Smart probe adaptor kit 1 9321000

Stainless steel sample adapter kit 1 6786600

Sodium hydroxide solution, 1 N (5%) 900 mL 104553

Sodium hydroxide solution, 1 N (5%) 3.60 L 104517

Reagents and standard solutions

Description Quantity Item no.

Silica reagent kit, includes:

Reagent 1–4, Standard 1

1 2035600

Reagent 1 Silica, 9610sc 2 L 2035702

Reagent 2 Silica, 9610sc 2 L 2035802

Reagent 3 Silica, 9610sc 2 L 2036002

Reagent 4 Silica, 9610sc 2 L 2037502

Standard 1 Silica, 9610sc 2 L 2035902

LR Phosphate reagent kit, includes:

Reagent 1–3, Standard 1-2

1 2036100

Reagent 1 LR Phosphate, 9611sc 2 L 2036202

Reagent 2 LR Phosphate, 9611sc 2 L 2036302

Reagent 3 LR Phosphate, 9611sc 2 L 2036502

Standard 1 LR Phosphate, 9611sc 2 L 2036602

Standard 2 LR Phosphate, 9611sc 2 L 2036402

HR Phosphate reagent kit, includes:

Reagent 1–3, Standard 1

1 6776100

Reagent 1 HR Phosphate, 9611sc 2 L 2036802

Reagent 2 HR Phosphate, 9611sc 2 L 2036902

Reagent 3 HR Phosphate, 9611sc 2 L 2037002

Standard 1 HR Phosphate, 9611sc 2 L 2037102

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Inhaltsverzeichnis

Wartungsplan auf Seite 18 Austauschen der Analysatorflaschen auf Seite 22

Den Analysator in den Abschaltmodus schalten

auf Seite 19

Fehlerbehebung auf Seite 25

Reinigen des Geräts auf Seite 19 Ersatzteile und Zubehör auf Seite 31

Sicherheitshinweise

Allgemeine Sicherheitshinweise, Gefahren- und Warnetikettenbeschreibungen finden Sie im

Installationshandbuch.

Wartung

G E F A H R

Mehrere Gefahren. Nur qualifiziertes Personal sollte die in diesem Kapitel des Dokuments

beschriebenen Aufgaben durchführen.

Wartungsplan

Tabelle 1 zeigt den empfohlenen Wartungsplan. Je nach Anforderungen der Anlage und den

Betriebsbedingungen kann es erforderlich sein, einige Aufgaben häufiger auszuführen.

Tabelle 1 Wartungsplan

Maßnahme 30 Tage 60 Tage 90 Tage 365 Tage

Reinigen der externen Oberflächen (Reinigen des

Geräts auf Seite 19).

X

Reinigen der Probenküvette (Reinigen der

Probenzelle auf Seite 20).

X oder nach

Bedarf

Ersetzen der Reagenzien (Austauschen der

Analysatorflaschen auf Seite 22).

X

1

X

2

Ersetzen der Standards (Austauschen der

Analysatorflaschen auf Seite 22).

X

3

Reinigen oder Ersetzen des Probenfilters (Y-Sieb) X oder nach Bedarf

Austausch der Luftfilter X oder nach Bedarf

Ersetzen des Reagenzluftfilters X

Ersetzen der Schläuche X

Ersetzen des Rührbolzens X

Ersetzen der Probenzelle X

1

Bei 10-Minuten-Zyklen

2

Bei 15-Minuten-Zyklen

3

Bei einer Kalibrierung pro Woche

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Wartungsinformationen anzeigen

Verwenden Sie das Menü WARTUNG, um den Wartungsverlauf für die Geräteteile anzuzeigen oder

zurückzusetzen.

1. Drücken Sie auf Diag.

2. Wählen Sie WARTUNG.

3. Wählen Sie eine Option.

Optionen Beschreibung

TEIL WARTEN Zeigt eine Liste mit Teilen und das Datum der zuletzt durchgeführten Wartung, das

Datum der nächsten Wartung und die Anzahl von Tagen bis zur nächsten fälligen

Wartung an. Starten Sie den Zähler für die nächste Wartung neu.

TEILEINFORMATION Zeigt das Datum an, an dem die einzelnen Teile in Betrieb genommen wurden, und

die Gesamtdauer, während der die einzelnen Teile betrieben wurden. Bei einigen

Teilen werden zusätzliche Informationen angezeigt.

NÄCHSTE WARTUNG Zeigt den Namen des Wartungsteils, das Datum der zuletzt durchgeführten

Wartung, das Datum der nächsten Wartung und die Anzahl von Tagen bis zur

nächsten fälligen Wartung an.

WARTUNGSVERL. Zeigt den Typ, das Datum und die Uhrzeit der letzten Wartung an.

Den Analysator in den Abschaltmodus schalten

Stoppen Sie den Analysator vor Beginn von Wartungsaufgaben. Wenn der Analysator gestoppt ist,

wird die Kolorimeterzelle gespült, danach werden der Probendurchfluss, der Mischermotor, die

Druckluftpumpe und die Heizung ausgeschaltet. Die Controller-Menüs bleiben aktiv.

1. Drücken Sie auf Menü.

2. Wählen Sie ANALYSATOR STOPPEN und dann JA, um den Vorgang zu bestätigen.

Hinweis: Wenn ANALYSATOR STARTEN angezeigt wird, befindet sich der Analysator bereits im

Abschaltmodus.

3. Warten Sie, bis der Status „100 % abgeschlossen“ anzeigt.

4. Schließen Sie die Absperrventile in den Probenleitungen, und schließen Sie dann die

Wartungsarbeiten ab.

Analysator wieder in Betrieb nehmen

Starten Sie nach Abschluss der Wartungsaufgaben den Analysator.

1. Stellen Sie sicher, dass alle Schläuche angeschlossen sind und dass die untere Tür geschlossen

und verriegelt ist.

2. Öffnen Sie die Absperrventile in den Probenleitungen.

3. Drücken Sie auf Menü.

4. Wählen Sie ANALYSATOR STARTEN.

Der Analysator startet den Normalbetrieb.

Reinigen des Geräts

H I N W E I S

Verwenden Sie zum Reinigen des Geräts, einschließlich von Display und Zubehör, keine Reinigungsmittel wie

Terpentin, Azeton oder ähnliche Produkte.

Reinigen Sie das Gerät mit einer milden Seifenlösung und einem feuchten Tuch.

Deutsch

19

Reinigen von Spritzern

V O R S I C H T

Gefahr von Kontakt mit Chemikalien. Entsorgen Sie Chemikalien und Abfälle gemäß lokalen,

regionalen und nationalen Vorschriften.

1. Befolgen Sie alle örtlichen Sicherheitsprotokolle zur Verschüttungskontrolle

2. Entsorgen Sie die Abfälle gemäß den zutreffenden Vorschriften.

Reinigung der Probenleitungen und Ventile

V O R S I C H T

Gefahr von Kontakt mit Chemikalien. Halten Sie sich an die Sicherheitsmaßnahmen im Labor, und

tragen Sie Schutzkleidung entsprechend den Chemikalien, mit denen Sie arbeiten. Beachten Sie die

Sicherheitsprotokolle in den aktuellen Materialsicherheitsdatenblättern (MSDS/SDB).

Neue Schläuche, Ventile und andere Probenaufbereitungsgeräte können mit Substanzen auf

Kieselsäurebasis (Öle, Staub) verschmutzt sein. Diese können zu etwas erhöhten Messwerten

führen, bis sie gereinigt wurden.

1. Spülen Sie ein bis zwei Stunden lang die Probenleitung mit der Probe.

2. Hierfür wird empfohlen, ein bis vier Liter einer verdünnten Lauge, beispielsweis eine 1N-

Natriumhydroxidlösung (5 %), in das vordere Ende der Probenleitung zu injizieren. Forcieren Sie

die Lösung durch den Analysator, um die Bauteile des Probensystems zu reinigen.

Reinigen der Probenzelle

V O R S I C H T

Gefahr von Kontakt mit Chemikalien. Halten Sie sich an die Sicherheitsmaßnahmen im Labor, und

tragen Sie Schutzkleidung entsprechend den Chemikalien, mit denen Sie arbeiten. Beachten Sie die

Sicherheitsprotokolle in den aktuellen Materialsicherheitsdatenblättern (MSDS/SDB).

Schalten Sie den Analysator in den Abschaltmodus. Siehe Den Analysator in den Abschaltmodus

schalten auf Seite 19.

Reinigen Sie nach Bedarf die Probenküvette im Kolorimeter. Siehe Abbildung 1 und Abbildung 2.

Zusätzlich erforderliche Artikel:

• Wattestäbchen mit Holz- oder Papierstab. Verwenden Sie keine Wattestäbchen mit

Kunststoffröhrchen.

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